For this batch I used 69% nitric mixed with 3 parts water. I added the iron turnings and let it sit for about 3 days. Some iron was still left in the bottom of the bottle. I strained it thru a tee shirt and tried it, way too dark for me. I added 2 more parts water to dilute it and it works great. So far I've used it on 2 maple guns and just did a ash stock today.
The difference in this batch was I used cast iron. Some told me not to use it but the Mad Monk said it would be fine. I tried it and he was right, best color I ever had. A nice brown with a dark reddish tint. And yes, I used USA made Grade 30 cast iron.
Bill